By C. F. Van Sumere, W. Van Brussel, K. Vante Casteele (auth.), Tony Swain, Jeffrey B. Harbone, Chris F. Van Sumere (eds.)
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Extra resources for Biochemistry of Plant Phenolics
HPLC has recently also been introduced for the detection of anthraquinones in plant material of various kinds 71 . Rai et al. 71 found that Corasil type II with gradient cyclohexane to ethyl acetate provided a superior resolution of anthraquinone mixtures. Again the retention times were directly related to the polarity of the compounds. The high-pressure liquid chromatography SEPARATION OF PLANT PHENOLICS 23 of xanthones from Gentianaceae and especially those which are poorly separated by the other chromatographic methods have been investigated by Hostettmann and Jacot-Guillarmod41 ,42.
J. H. Looker. 1975. J. Org. Chem. , Y. Terui, K. Tori, N. Tsuji. 1976. Tetrahedron Letters 8: 619.
J. Chromatogr . 1£(2): 93. 271-79. Yang, S. , J. K. Selkirk, E. V. Plotkin and H. V. Gelboin. 1975. Cane. Res. 35: 3642-50. ADVANCES IN THE SPECTROSCOPY OF PLANT PHENOLICS V. M. CHARI and H. WAGNER Institut fUr Pharmazeutische Arzneimittellehre der Universitat Mlinchen, Mlinchen, Germany Introduction UV Spectroscopy Mass Spectrometry lH_NMR Spectroscopy Solvent Induced Shifts Lanthanide Induced Shifts Nuclear Overhauser Effect Electron Paramagnetic Resonance 13c-NMR Spectroscopy References INTRODUCTION During the classical period of the study of natural products, the molecular structures of such substances were unravelled by skilful application of chemical degradative methods.